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Beilstein J. Org. Chem. 2016, 12, 353–361, doi:10.3762/bjoc.12.39
Graphical Abstract
Figure 1: Structures of targeted synthetic inositol derivatives.
Scheme 1: Synthesis of O-alkylated inositol derivatives 1. Reagents and conditions: a) NaBH4, iPrOH, rt, 2 h,...
Scheme 2: Synthesis of O-alkylated fluorinated inositol derivatives 2.
Scheme 3: Synthesis of C-alkenylated inositol intermediates.
Figure 2: nOe correlations for C-alkenylated inositol intermediates.
Scheme 4: Synthesis of C-branched inositol derivatives 3 and 4.
Scheme 5: Synthesis of C-branched fluorinated inositol derivatives 5. Reagents and conditions: a) TrCl, DMAP ...
Scheme 6: Synthesis of C-branched fluorinated inositol derivatives 6. Reagents and conditions: a) TrCl, DMAP ...